水性聚氨酯乳液的制备装置的制作方法

文档序号:18262853发布日期:2019-07-24 13:16
水性聚氨酯乳液的制备装置的制作方法

本发明属于水性聚氨酯乳液生产设备技术领域,特别涉及一种水性聚氨酯乳液的制备装置。



背景技术:

水性聚氨酯是以水代替有机溶剂作为分散介质的新型聚氨酯体系,也称水分散聚氨酯、水系聚氨酯或水基聚氨酯;水性聚氨酯以水为溶剂,无污染、安全可靠、机械性能优良、相容性好、易于改性等优点。水性聚氨酯可广泛应用于皮革涂饰剂。

水性聚氨酯的制备方法通??煞治馊榛ê湍谌榛街?。外乳化法是指采用外加乳化剂,在强剪切力作用下强制性地将聚氨酯粒子分散于水中的方法,但因该法存在乳化剂用量大、反应时间长以及乳液颗粒粗、最终得到的产品质量差、胶层物理机械性能不好等缺点,因而目前生产基本不用该法。内乳化法又称自乳化法,是指在聚氨酯分子结构中引人亲水基团无需乳化剂即可使自身分散成乳液的方法,因此成为目前水性聚氨酯生产和研究采用的主要方法.内乳化法又可分为丙酮法、预聚体混合法、熔融分散法、酮亚胺/酮联氮法、?;ざ嘶榛?。

采用现有的制备装置,由于反应程度难以控制,导致水性聚氨酯乳液的状态不稳定,难以制备出高质量的水性聚氨酯乳液。



技术实现要素:

本发明解决现有技术中存在的上述技术问题,提供一种水性聚氨酯乳液的制备装置。

为解决上述问题,本发明的技术方案如下:

水性聚氨酯乳液的制备装置,包括壳体;

所述壳体内包括引流罩;所述引流罩上部为半球形、下部为圆柱形筒体;所述引流罩顶部设置溢流槽;

所述壳体底部设置搅拌电机,与所述搅拌电机的连接的旋转轴竖直伸入所述引流罩内,所述引流罩通过固定杆固定在旋转轴上;所述旋转轴上还设置有旋转叶片,所述旋转叶片位于引流罩下方;

所述壳体侧壁设置有储液槽,所述储液槽与第二进液管相连,所述储液槽的外壁设置有喷头,所述喷头的喷液方向指向引流罩外壁;所述第二进液管上设置液体加压泵;

所述溢流槽正上方设置第一进液管。

作为本发明的一种改进,所述引流罩的内壁上部设置有加热元件,所述加热元件下方设置液位报警器??墒实倍砸髡滞獗诹魈实囊禾褰屑尤?,控制反应的进行,同时设置液位报警器,避免引流罩内液位过高,影响加热元件的使用。

作为本发明的一种改进,所述引流罩的顶部设置有快速接头,所述快速接头上方、壳体顶部设置通气管,所述通气管上设置压力控制阀,所述通气管与壳体连接处设置密封垫圈。移动通气管,使得其与快速接头相连接,打开压力控制阀,对引流罩内部进行加压和降压,进一步增加液体在竖直方向上的对流。

作为本发明的一种改进,所述引流罩内壁的下部设置垂直于内壁的刀片,所述刀片均匀分布在同一高度上。当液面高于刀片高度时,可对混合乳液进行剪切。

作为本发明的一种改进,所述壳体底部设置出料口。便于出料。

相对于现有技术,本发明的优点如下,

本发明的水性聚氨酯乳液的制备装置通过设置引流罩上的溢流槽,使得从第一进液管进入的第一原料从引流罩外壁均匀流淌,通过设置储液槽和喷头,使得从第二进液管进入的第二原料均匀喷洒在旋转的引流罩的外壁,使得两种原料可均匀接触的同时,可控制反应的进程,制得高质量的水性聚氨酯乳液。

附图说明

图1为水性聚氨酯乳液的制备装置结构示意图;

图中:1是壳体、2是引流罩、3是溢流槽、4是搅拌电机、5是旋转轴、6是固定杆、7是旋转叶片、8是储液槽、9是第二进液管、10是喷头、11是液体加压泵、12是第一进液管、13是加热元件、14是液位报警器、15是快速接头、16是通气管、17是压力控制阀、18是密封垫圈、19是刀片、20是出料口。

具体实施方式

实施例1:

参见图1,水性聚氨酯乳液的制备装置,包括壳体1;

所述壳体1内包括引流罩2;所述引流罩2上部为半球形、下部为圆柱形筒体;所述引流罩2顶部设置溢流槽3;

所述壳体1底部设置搅拌电机4,与所述搅拌电机4的连接的旋转轴5竖直伸入所述引流罩2内,所述引流罩2通过固定杆6固定在旋转轴5上;所述旋转轴5上还设置有旋转叶片7,所述旋转叶片7位于引流罩2下方;

所述壳体1侧壁设置有储液槽8,所述储液槽8与第二进液管9相连,所述储液槽8的外壁设置有喷头10,所述喷头10的喷液方向指向引流罩2外壁;所述第二进液管9上设置液体加压泵11;

所述溢流槽3正上方设置第一进液管12。

实施例2:

参见图1,作为本发明的一种改进,所述引流罩2的内壁上部设置有加热元件13,所述加热元件13下方设置液位报警器14??墒实倍砸髡?外壁流淌的液体进行加热,控制反应的进行,同时设置液位报警器14,避免引流罩2内液位过高,影响加热元件13的使用。

实施例3:

参见图1,作为本发明的一种改进,所述引流罩2的顶部设置有快速接头15,所述快速接头15上方、壳体1顶部设置通气管16,所述通气管16上设置压力控制阀17,所述通气管16与壳体1连接处设置密封垫圈18。移动通气管16,使得其与快速接头15相连接,打开压力控制阀17,对引流罩2内部进行加压和降压,进一步增加液体在竖直方向上的对流。

实施例4:

参见图1,作为本发明的一种改进,所述引流罩2内壁的下部设置垂直于内壁的刀片19,所述刀片19均匀分布在同一高度上。当液面高于刀片19高度时,可对混合乳液进行剪切。

实施例5:

参见图1,作为本发明的一种改进,所述壳体1底部设置出料口20。便于出料。

本发明还可以将实施例2、3、4、5所述技术特征中的至少一个与实施例1组合形成新的实施方式。

需要说明的是上述实施例仅仅是本发明的较佳实施例,并没有用来限定本发明的?;し段?,在上述基础上做出的等同替换或者替代均属于本发明的?;し段?。

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