有机化学装置的制造及其处理,应用技术
  • 本发明涉及的是新化合物及这些化合物与金属的新配合物。本发明的新化合物及配合物可用于疾病的诊断和治疗方法。金属配合物,如含放射性金属的那些配合物作为诊断试剂和治疗剂正在有发现越来越多的用途。其中特别令人感兴趣的是那些含有能够被所需部位选择性吸收以便于评定和治疗受试体的生物活性部分的配合物。本...
  • 本发明涉及生产包括紫杉醇的紫杉烷型双萜的方法,紫杉醇是用于治疗卵巢癌、乳癌、肺癌等的很好的药剂。用于卵巢癌、乳癌、肺癌等的治疗药剂的紫杉醇是一种从短叶紫杉NUTT中分离出来后被鉴别出的紫杉烷(taxane)型双萜,紫杉是一种属于紫杉属紫杉科族的植物,紫杉醇有一个与上述药理活性有关的复杂的酯基??梢?..
  • 本发明涉及在催化剂存在下、水溶液中水合不饱合醛制造羟基烷醛的方法。以往,作为将不饱和醛之一的丙烯醛在催化剂存在下,水溶液中进行水合,制取羟基烷醛之一的3-羟基丙醛方法有以下的各种制造方法。即,在USP2,434,110号中公开了使用硫酸等的无机酸作为上述反应系统中酸性均相催化剂的方法。但是这种方法...
  • 本发明涉及在液态氨中由二苯酮制备二苯酮亚胺的方法。在熔融形式的或在溶液中的二苯酮与气态或液态氨的直接反应中,作为催化剂必须加入氯化铁(III)(JP-A-61/030563,产率57%)、有机酸,如苯甲酸(US-A-4130586,产率18-65%)或氯化铵(SyntheticCommunica...
  • 本发明涉及如下通式的哌嗪衍生物,互变异构体,立体异构体,包括其混合物及其盐,特别是具有药物可接受的酸或碱的盐,它们具有有效的药理性能,尤其是抑制聚集作用的效果,本发明还涉及含这些化合物的药物组合物及其用途以及其制备方法。在上述通式I中的先决条件是假若Ra表示4-吡啶基时,则不可能同时(a)Y1表...
  • 本发明涉及具有骨生成促进活性、骨吸收抑制活性和其他活性的光学活性苯并硫杂庚英衍生物,和含有其作为活性成分的骨疾病预防或治疗药物。骨疾病是一种涉及由骨量减少超过某一程度引起的某些症状或倾向的病理状态或疾病。骨质疏松(一种骨疾病)的主要症状是脊柱后凸,和背腰骨、椎骨体、股骨颈、桡骨下端、肋骨、肱骨上端...
  • 本发明涉及从含(甲基)丙烯酸和沸点高于(甲基)丙烯酸的惰性疏水有机液体为主要成分和还含有低级醛为次要成分的混合物中精馏分离(甲基)丙烯酸的新方法。(甲基)丙烯酸是简写,表示丙烯酸或甲基丙烯酸。(甲基)丙烯酸本身或它的各种形式的酯对制备具有非常广泛用途,例如粘合剂的聚合物是特别重要的。(甲基)丙烯酸...
  • 本发明涉及制备丙烯酸的方法,尤其,本发明涉及一种在特定条件下制得的钼/钒基氧化物催化剂存在下,使用分子氧或含分子氧的气体,通过气相催化氧化丙烯醛或含丙烯醛的气体来制备丙烯酸的方法。多种改进的催化剂被推荐用于通过气相催化氧化丙烯醛来有效地制备丙烯酸。其中大多数量是含钼和钒作为主要成分的钼/钒基催化剂...
  • 本发明涉及用于异丁烯醛气相氧化制备异丁烯酸的新催化剂,异丁烯醛是通过异丁烯或叔丁醇气相催化氧化得到的。据报道,有多种催化剂可作为异丁烯醛气相氧化制备异丁烯酸的催化剂,尤其是在许多专利公开出版物中报道了杂多酸衍生物作为制备异丁烯酸的催化剂。然而,由于包括杂多酸衍生物的催化剂自身的性质,使它们具有一些...
  • 本发明是属于合成气一步制取二甲醚的方法,特别是所用的催化剂及其制备过程。二甲醚不仅是从合成气经由甲醇转化制汽油改良法的主要中间体,而且是生产多种化工产品的重要原料,并在制药、染料、农药等工业中有许多独特的用途。二甲醚还可能作为一种城市煤气或液化气甚至柴油的代用品而日益引起重视。由合成气一步制取二甲...
  • 本发明涉及借助1,1-二氟四卤代乙烷与醇的反应直接制备卤代二氟乙酸烷基酯的方法。卤代二氟乙酸烷基酯是合成药物和植物保健产品的中间体?;竦谜庑┞贝宜嵬榛サ姆椒ㄒ丫窃亓撕芏?。这些方法中最普遍采用的是醇与卤代二氟乙酸反应,或优选与相应的氟化物和氯化物反应。根据大量的各种技术方法可以得到这些卤代...
  • 本发明涉及链烷磺酸的合成,具体地本发明的内容在于,由相应的含硫衍生物制备C1-C4链烷磺酸。链烷磺酸及其盐在工业上有许多应用,具体如洗涤剂,乳化剂,酯化催化剂,以及某些树脂的硬化剂。工业上,链烷磺酸往往是由链烷经磺化作用或氯磺化作用制备的。然而这两种合成方法的缺点是导致在烃链的不同碳原子上生成磺化...
  • 本发明涉及新的1-环丙基四唑啉酮,它们的制备方法,它们作为除草剂的用途,及其制备过程中新的中间体和它们的制备方法。已知某些取代的四唑啉酮具有除草活性[见美国专利4,618,365(=EP-A-146,279);4,826,529;4,830,661;4,956,469;5,003,075;5,01...
  • 本发明涉及一种,该方法包括由1,3-二氯苯经二硝基化得到1,3′-二氯-4,6/2,4-二硝基苯混合物,接着与苄醇钠(Sodiumbenzylate)反应得到1,3-二苄氧基-4,6-二硝基苯和催化氢化。4,6-二氨基间苯二酚是塑料的重要单体结构单元,特别是组成聚苯并噁唑的重要单体(高分子,19...
  • 本发明涉及1-氧代-2-(苯磺酰氨基)戊基哌啶衍生物,其制备方法及其药用。本发明化合物如下式(I)所示其中R1是氢或(C1-C4)烷基,R2是氢或直链或支链(C1-C4)烷基,R3是直链或支链(C1-C7)烷基,-(CH2)nOCH3基团(其中n是1,2或3)或-CH2O(C2H4O)mCH3(...
  • 本发明涉及D-氨基酸的立体控制合成方法。下式(1)代表D-氨基酸-N-(S)-α-烷基苄基酰胺中,R1是甲基、乙基或异丙基及R2是甲基或乙基的化合物是重要的物质,它们可用作具有强甜度的物质的中间体,见US.5286509中所述。所述式(1)如下式中标有*的碳原子具有D-氨基酸结构,R1是具有1至...
  • 本发明涉及由有机伯胺与碳酰氯在有机溶剂中、于60-100℃温度下反应,其中反应混合物通过泡罩塔进行循环。通过使有机伯胺与碳酰氯在有机溶剂中反应连续制备有机异氰酸酯的方法已在多处介绍过,并已大规模进行生产(例如,参见UllmannsEnzyklopdiederTechnischenChem...
  • 本发明涉及通式I的11β-芳基-4-雌烯及其药物上适宜的酸加成盐,以及它们的制备方法、含有该化合物的药物组合物、在制备药物上的应用和为此所需的新的中间产物,式中X表示氧原子,肟基N-OH或2个氢原子,R1表示氢原子或甲基,R2表示羟基,C1-C10-烷氧基-或C1-C10酰氧基,R3表示氢原子、...
  • 本发明涉及通过特定的缩合反应由醛制备β-酮醇的新方法以及此方法制得的一些新产物。ChemistryLetters1991,1377-1378(Inoue等人)披露了环状α-甲叉基碳酸酯即4,4-二甲基-5-甲叉基-1,3-二氧戊环-2-酮(以下称“环碳酸酯”)和芳醛之间环化加成反应,裂解掉二氧...
  • 本发明涉及可用于将氨基酸转化成卤代甲基酮然后又转化成氨基酸环氧化物的新方法。这样的环氧化物是合成肾素和HIV蛋白酶的抑制剂的重要的中间体。所述肾素和HIV蛋白酶的抑制剂尤其可用于治疗和/或预防HIV感染(AIDS)。氨基酸α-卤代甲基酮除可用作某些含半胱氨酸和丝氨酸的蛋白酶的不可逆的活性部位的抑制...
技术分类
手机购彩票有哪个平台最可靠
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